FAPAS (Gıda Kimyası)

2012 – 2013 FAPAS YETERLİK TESTLERİ PROGRAMI
Nisan 2012 – Mart 2013
Lütfen açıklamaları okuyunuz.
 FAPAS 2012-2013 Programını Program sayfalarında inceleyebilirsiniz.
Notlar
a)
b)
c)
d)
e)
İlginizi çekebilecek testleri daha kolay bulabilmeniz için indeks sayfasını kullanabilirsiniz.
Belirtilen dağıtım tarihleri planlanan tarihlerdir. Kayıt yaptıdırdığınız testlerden, herhangi bir sebeple
ertelenenler olduğu takdirde email ile tarafınıza bildirilecektir. Testlerin büyük bir bölümünün kapanış
tarihleri dağıtım tarihlerinden itibaren 6-8 haftadır.
Her test için test materyallerinin yaklaşık miktarları verilmiştir. Metodunuz daha fazla materyal
gerektiriyorsa lütfen ekstra test materyal sayısını bildiriniz. İlave test materyaller için ücret ödenir.
Ekstra test materyalleri ilave performans değerlendirmesi hakkı kazandırmaz. Birden fazla değerlendirme
için çoklu kayıt yaptırmanız gerekmektedir.
Test materyalleri DHL ile gönderilir.
 Kayıtlar:
FAPAS® Programına kayıtlar için Fera Standard Terms and Conditions for Proficiency Testing Schemes
dokümanında belirtilen şartlar geçerlidir. Dokümana www.fapas.com adresinden ulaşılabilir.
Notlar
a)
b)
30 gün içerisinde kayıt onayınız ulaşmazsa lütfen iletişime geçiniz.
Siparişiniz alındığında faturanız kesilecektir. Bu, ödemelerin testlerden önce yapılacağı anlamına
gelmektedir.
 İlave notlar:
i. Dağıtım
a)
b)
c)
d)
e)
Yukarıda da belirtildiği gibi, numuneler DHL ile gönderilmektedir. Bazı paketler sıcaklık değişimlerini
minimize etmek için buz bloklar içerir ancak soğuk araçlarda taşınmamaktadır. Numuneniz elinize
ulaştığında sıcaklığı yüksek de olsa, taşıma süresinin büyük bölümünde soğuk kaldığından dolayı testler için
uygundur.
Numuneniz dağıtımdan itibaren 4 gün içerisinde elinize ulaşmadığında lütfen iletişime geçiniz.
Numuneler gönderildiğinde, kayıtlı olan email adresine FAPAS tarafından DHL takip numarası “Airway Bill
Number” gönderilecektir.
Takip numaralarına kullanıcı adı ve şifrenizle girdiğiniz FAPAS web sitesindeki sayfanızdan da
ulaşabilirsiniz.
Numunelerin takibi katılımcı sorumluluğundadır.
ii. Gümrük
a)
Test materyallerinin gümrüklerdeki muhtemel hasar ve kayıplarından veya olası gümrük işlemlerinden FAPAS
sorumlu değildir.
iii. Sonuçlar
a)
b)
Katılımcıların sonuçları bildirmesi için numune dağıtım tarihinden itibaren genellikle 6 haftaları
bulunmaktadır. Bazı analizler test materyali ve/veya analitlerden kaynaklanan nedenlerden dolayı daha kısa
sürede tamamlanmalıdır. Bu testler programda belirtilmektedir.
Sonuçlar FAPAS® web sitesi üzerinden kabul edilmektedir.
iv. Raporlar
a)
b)
c)
Test fiyatlarına katılımcıların kullanıcı adı şifreleriyle giriş yaptığı sistemde görebileceği elektronik rapor
dahildir.
Raporlar genellikle testin kapanmasından 5 hafta sonra web sitesinde yayımlanır.
Raporlar PDF formatında ve dijital imzalı olarak sunulmaktadır. Görüntülemek için Adobe Reader 7 veya
üzeri gerekmektedir.
2012 – 2013 FAPAS YETERLİK TESTLERİ PROGRAMI
Nisan 2012 – Mart 2013
Index
3-MCPD & 1,3 DCP .......................... 2
chocolate .................................. 1, 6, 7
hazelnut (water/nut slurry) ................ 9
acesulfame-k .................................. 13
chocolate cake mix ......................... 11
hazelnut, hazelnut protein ................ 7
acidity ............................................. 14
cholesterol ...................................... 14
higher alcohols (sum) ......................13
acrylamide ........................................ 2
chromium........................................ 12
histamine ......................................6, 7
aflatoxins .......................................... 9
citric acid .................................. 11, 13
honey ........................................ 2, 4, 5
alcoholic strength ........................... 13
coccidiostats ................................. 4, 5
hot pepper sauce ............................11
almond ......................................... 7, 9
cocoa........................................ 10, 12
hydrogenated vegetable oil .............15
almond protein ................................. 7
cola drink ........................................ 13
hydroxymethylfurfural (HMF) ............ 2
aluminium ....................................... 12
colours ............................................ 13
hydroxyproline.................................. 1
animal (pork) fat ............................. 15
condensed milk................................. 1
illegal dyes ......................................11
animal feed................................. 9, 10
copper ........................................ 6, 12
immersion in ethanol ........................ 8
anisidine value ............................... 14
corn/maize ........................................ 1
immersion in olive oil ........................ 8
anthelmintics ................................ 4, 5
corned beef ...................................... 4
infant cereal ....................................12
antimony ........................................ 12
crab meat ....................................... 12
infant formula ............................ 12, 14
antioxidants .................................... 11
cranberry juice ................................ 13
infant soya formula ........................... 6
apple juice ................................ 10, 13
crispbread......................................... 2
instant coffee ..................................10
apple purée .............................. 10, 17
crude fibre ........................................ 6
iodine .......................................... 8, 14
apricot purée .................................. 17
cyanuric acid..................................... 2
iodine value.....................................14
arsenic ........................................... 12
cyclamate ....................................... 13
iron.......................................... 6, 8, 12
arsenic, inorganic ........................... 12
dairy ration........................................ 6
jam .............................................. 7, 11
ash ............................................... 1, 6
deoxynivalenol (DON) ..................... 10
k232 & k270 ....................................14
aspartame ...................................... 13
diastase ............................................ 2
lactose ............................................. 1
avermectins .................................. 4, 5
dihydrostreptomycin.......................... 5
lamb ................................................. 3
barley flour ..................................... 10
DON ................................................. 9
LC-PUFAs.......................................14
beef .................................................. 3
dried apricot .................................... 11
lead ............................................. 6, 12
benzoic acid ............................. 11, 13
dried figs ........................................... 9
lemon purée ....................................17
beta-agonists.................................... 4
dried vine fruit ................................. 10
lettuce purée ............................... 3, 17
beta-lactams................................. 4, 5
edible oil ......................................... 12
leucomalachite green ....................... 4
biscuits ............................................. 2
egg ................................................... 7
liquid vitamin supplement ................11
bisphenol A ...................................... 8
egg, egg white protein ...................... 6
magesium ........................................ 6
bovine milk ....................................... 5
eggs ................................................. 5
magnesium ............................. 6, 8, 13
bovine muscle .................................. 4
ELISA ....................................... 6, 7, 9
maize ............................................... 9
bovine urine...................................... 5
energy drink ...................................... 8
maize flour ................................ 10, 16
brandy ............................................ 13
esters of 3-MCPD ............................. 2
manganese ...................................6, 8
bread ................................................ 1
ethyl acetate ................................... 13
meat............................................ 3, 11
breadcrumbs .................................... 1
ethyl carbamate .............................. 13
melamine ......................................2, 8
breakfast cereal .................... 8, 10, 11
fatty acids ....................................... 14
melon purée ....................................17
brix ........................................... 11, 13
fish............................ 1, 3, 4, 6, 12, 14
mercury ...........................................12
butyric acid ................................. 1, 14
fish identification ............................... 3
mercury, methyl ..............................12
cabbage purée ........................... 3, 17
fish muscle ....................................... 4
methanol .........................................13
cadmium ........................................ 12
fish oil ............................................. 14
methylbutanol..................................13
caffeine .................................... 11, 13
fish paste .......................................... 1
milk ...............................................6, 7
cake mix ....................................... 6, 7
fluoroquinolones ........................... 4, 5
milk powder ......... 2, 3, 8, 9, 11, 12, 15
calcium ................................... 6, 8, 13
food simulant .................................... 8
mixed fat spread .............................14
canned fish ................................... 6, 7
formaldehyde .................................... 8
moisture .................................... 1, 2, 6
canned meat ................................ 1, 8
fructose....................................... 2, 13
molybdenum ...................................12
canned meat meal ............................ 1
fruit juice ......................................... 12
nitrate............................................... 3
cephalosporins ................................. 5
fruit purée ....................................... 11
nitrite ................................................ 3
cereal .......................... 1, 9, 10, 14, 16
fumonisins .................................. 9, 10
nitrofuran metabolites ....................... 5
cheese ............................................. 1
ginger (spice) .................................... 9
nitrofurans .....................................4, 5
chicken ............................................. 3
glucose ....................................... 2, 13
nitrogen ............................................ 1
chicken muscle ................................. 5
gluten ........................................... 6, 7
non-fat solids ................................... 1
chilli powder ............................... 9, 12
grape purée .................................... 17
non-permitted colours .....................11
chilli sugar paste............................. 12
grapefruit juice ................................ 13
NSAIDs .........................................4, 5
chloramphenicol ........................... 4, 5
green bean (inc pods) purée ........... 17
NSP fibre ......................................... 1
chloride ...................................... 1, 11
green coffee ................................... 10
nut contamination ............................. 7
chlormequat ................................... 16
ground coffee.................................. 13
nutritionally fortified oil.....................14
®
FAPAS 2011-12 (Index) – Rev: 20111116
Sayfa 1 / 2
2012 – 2013 FAPAS YETERLİK TESTLERİ PROGRAMI
Nisan 2012 – Mart 2013
nylon film .......................................... 8
powdered baby food ....................... 11
thyrostats ......................................4, 5
oat flour .......................................... 10
powdered rice ................................. 12
tin....................................................12
ochratoxin A ................................... 10
prawns .......................................... 4, 5
titratable acidity ................................ 1
oil ............................................... 8, 11
premix .............................................. 6
tomato paste ...................................12
oily fish ........................................... 15
protein .............................................. 6
tomato purée ...................................17
olive oil ..............................7, 8, 14, 15
quinine ............................................ 13
tomato sauce ..................................11
omega-3 & omega-6 ....................... 14
quinolones .................................... 4, 5
tonic water ......................................13
orange juice.................................... 13
quinolones & fluoroquinolones ...... 4, 5
total acidity ................................ 11, 13
orange purée .................................. 17
refined palm oil ................................. 2
total dietary fibre .............................. 1
OTA ................................................. 9
rice ................................................... 9
total fat ........................................ 1, 14
overall migration ............................... 8
rice (brown) .................................... 16
total folate .......................................11
PAHs ................................................ 7
roasted coffee ................................. 10
total malachite green ........................ 4
PAHs (EU priority) ............................ 7
saccharin ........................................ 13
total niacin.......................................11
palm oil............................................. 7
saturated FAs ................................. 14
total oil ............................................. 6
paprika ........................................... 10
selenium ................................. 6, 8, 12
total primary aromatic amines .......... 8
patulin ............................................ 10
sheep feed........................................ 6
total SO2 .........................................13
peanut .......................................... 6, 9
smoked meat .................................... 7
total sugars ....................... 1, 6, 11, 13
peanut, peanut protein...................... 6
snack food ........................................ 1
total volatile basic nitrogen (TVB-N) . 1
pear purée ...................................... 17
sodium .............................. 1, 6, 11, 13
trans fatty acids ...............................14
penicillins ......................................... 5
soft drink ................................... 12, 13
trifluralin (single herbicide) ..............15
permitted colours ............................ 11
sorbic acid ................................ 11, 13
TVB-Nitrogen ................................... 1
peroxide value ................................ 14
soy sauce ......................................... 2
unsaturated FAs, mono ...................14
pesticide residues.......... 15, 16, 17, 18
soya flour ........................................ 12
unsaturated FAs, poly .....................14
pH ............................................ 11, 13
soya, soya protein............................. 7
vegetable oil ....................................14
phosphoric acid (as P2O5)............... 13
spinach purée ................................... 3
vegetable purée ..............................12
phosphorus ............................ 6, 8, 13
starch ........................................... 1, 6
veterinary drug residues ................4, 5
photo initiators .................................. 8
strawberry purée ............................. 17
vine fruit ..........................................17
phthlates .......................................... 8
sucrose ................................. 2, 11, 13
vitamins ...................................... 6, 11
pig kidney ......................................... 4
sugar confectionary ........................ 11
volatile acidity..................................13
pig liver............................................. 4
sulfonamides ................................ 4, 5
wheat flour ........................ 1, 7, 10, 16
pig ration .......................................... 6
sulphites ....................................... 6, 7
whisky .............................................13
pistachio (water/nut slurry)................ 9
sulphur dioxide ............................... 11
wine .................................... 10, 12, 13
plastic film ........................................ 8
sweet (bell) pepper purée ............... 17
zearalenone (ZON) .........................10
pork .................................................. 3
synthetic hormones....................... 4, 5
zinc ......................................... 6, 8, 12
porridge oats .................................... 1
T-2 & HT-2 toxins............................ 10
ZON ................................................. 9
potassium ................................... 8, 13
tea .................................................. 17
β-agonists .....................................4, 5
potato purée ................................... 17
tetracyclines ................................. 4, 5
poultry ration .................................... 6
theobromine ................................... 11
®
FAPAS 2011-12 (Index) – Rev: 20111116
Sayfa 2 / 2
FAPAS PROGRAMME & PROFICIENCY TEST ORDER FORM
APRIL 2012 – MARCH 2013
Besin Bileşenleri
dispatch
date
test details
place order
approx. 
quantity
dd/mm/yyyy
code
matrix
analyte
12/04/2012
0179
canned meat
moisture, ash, total fat, nitrogen,
sodium & chloride
150 g
13/06/2012
0180
canned meat
meal
moisture, ash, total fat, nitrogen,
sodium & chloride
150 g
23/08/2012
0181
canned meat
moisture, ash, total fat, nitrogen, hydroxyproline
150 g
17/10/2012
0182
canned meat
moisture, ash, total fat, nitrogen, hydroxyproline
150 g
04/01/2013
0183
canned meat
meal
moisture, ash, total fat, nitrogen,
sodium, chloride, total sugars
150 g
27/02/2013
0184
canned meat
moisture, ash, total fat, nitrogen,
sodium, chloride
150 g
02/05/2012
2446
wheat flour
moisture at 130C, ash, nitrogen &
total dietary fibre by AOAC
150 g
07/06/2012
2447
porridge oats
moisture at 130C, ash, total fat, nitrogen,
total dietary fibre by AOAC &
NSP fibre by Englyst
150 g
16/08/2012
2448
bread
sodium,
50 g
o
27/09/2012
2449
cereal
moisture at 130 C, ash, nitrogen &
total dietary fibre by AOAC
150 g
31/01/2013
2450
breadcrumbs
moisture, ash, nitrogen, starch &
total dietary fibre by AOAC
150 g
24/05/2012
2598
corn/maize snack
food
moisture, ash, total fat, nitrogen,
sodium & chloride
50 g
03/07/2012
2599
fish paste
moisture, ash, total fat, nitrogen,
sodium & chloride
150 g
01/08/2012
25100
canned fish
total volatile basic nitrogen (TVB-N)
150 g
30/08/2012
25101
condensed milk
moisture, ash, total fat, nitrogen & total sugars
150 mL
29/10/2012
25102
chocolate
moisture, total fat, butyric acid,
lactose & sucrose
150 g
16/11/2012
25103
milk powder
moisture, ash, total fat, nitrogen,
titratable acidity & lactose
50 g
25/01/2013
25104
infant formula
moisture, ash, total fat, nitrogen & lactose
50 g
13/02/2013
25105
cheese & pasta
meal
moisture, ash, total fat, nitrogen,
sodium & chloride
100 g
26/02/2013
25106
butter
moisture, total fat, non-fat solids, pH & chloride
200 g
20/03/2013
25107
canned fish
total volatile basic nitrogen (TVB-N)
150 g
sample contact
name & email
Dipnotlar
total sugars = titrasyon metodu sonucu (ör. Layne-Eynon, Luff-Schoorl, Munson Walker) veya HPLC ile yapıldıysa,
fruktoz, glikoz, sakkaroz, laktoz, galaktoz ve maltoz toplamı.
®
FAPAS 2012-13 (Program) – Rev: 20111116
Sayfa 1 / 18
extra
TMs
FAPAS PROGRAMME & PROFICIENCY TEST ORDER FORM
APRIL 2012 – MARCH 2013
Acrylamide / Melamine / 3-MCPD
dispatch
date
test details
place order
approx. 
quantity
dd/mm/yyyy
code
matrix
analyte
18/04/2012
3034
milk powder
melamine & cyanuric acid
(low levels, <5 mg/kg)
50 g
10/07/2012
3035
crispbread
acrylamide
50 g
26/09/2012
3036
animal feed
melamine & cyanuric acid
50 g
19/10/2012
3037
biscuits
acrylamide
50 g
21/02/2013
3038
milk powder
melamine and cyanuric acid (> 5mg/kg)
50 g
25/05/2012
2633
soy sauce
3-MCPD & 1,3 DCP
40 g
20/09/2012
2634
refined palm oil
esters of 3-MCPD
50 mL
09/01/2013
2635
hydrolysed
vegetable protein
3-MCPD & 1,3 DCP
40 g
14/03/2013
2636
soy sauce
3-MCPD & 1,3 DCP
40 g
sample contact
name & email
extra
TMs
Bal
dispatch
date
test details
place order
approx. 
quantity
dd/mm/yyyy
code
matrix
analyte
17/07/2012
2824
honey
moisture, fructose, glucose, sucrose,
hydroxymethylfurfural (HMF) & diastase
100 g
15/01/2013
2825
honey
fructose, glucose, sucrose, hydroxymethylfurfural
(HMF) & diastase
100 g
a
Dipnotlar
a
bu test materyali tağşişli bal olabilir.
®
FAPAS 2012-13 (Program) – Rev: 20111116
Sayfa 2 / 18
sample contact
name & email
extra
TMs
FAPAS PROGRAMME & PROFICIENCY TEST ORDER FORM
APRIL 2012 – MARCH 2013
Authenticity
dispatch
date
test details
place order
approx. 
quantity
dd/mm/yyyy
code
matrix
analyte
13/04/2012
2945
D
chicken
adulteration/contamination (presence/absence) of
matrix with one or more from: beef, lamb or pork
30 g
19/07/2012
2946
D
lamb
adulteration/contamination (presence/absence) of
matrix with one or more from: beef, chicken or pork
30 g
18/09/2012
2947
fish
identification of unknown fish (3 samples) selected
from the following list:
Gadus morhua, (Linnaeus 1758)
Limanda limanda, (Linnaeus 1758)
Melanogrammus aeglefinus, (Linnaeus 1758)
Merluccius merluccius, (Linnaeus 1758)
Hippoglossus hippoglossus, (Linnaeus 1758)
Pleuronectes platessa, (Linnaeus 1758)
Pollachius virens, (Linnaeus 1758)
Merlangius merlangus, (Linnaeus 1758)
3 x 10 g
04/12/2012
2948
processed food
adulteration/contamination (presence/absence) of
matrix (2 samples) with pork
2 x 30 g
15/02/2013
2949
beef
adulteration/contamination (presence/absence) of
matrix with one or more from: chicken, lamb or pork
30 g
D
sample contact
name & email
extra
TMs
Nitrate & Nitrite
dispatch
date
test details
place order
approx. 
quantity
dd/mm/yyyy
code
matrix
analyte
25/04/2012
1580
meat
nitrate & nitrite
25 g
18/06/2012
1581
cabbage purée
nitrate
70 g
13/08/2012
1582
lettuce purée
nitrate
70 g
12/10/2012
1583

milk powder
nitrate & nitrite (low level)
40 g
16/11/2012
1584
meat
nitrate & nitrite
25 g
24/01/2013
1585

feeding stuff
nitrite
40 g
12/02/2013
1586
spinach purée
nitrate
70 g
25/03/2013

meat
nitrate & nitrite
25 g
D

1587
dondurarak kurutulmuş (freeze dried) numune, analizden önce tekrar sulandırılmalıdır.
testin süresi kısadır
®
FAPAS 2012-13 (Program) – Rev: 20111116
Sayfa 3 / 18
sample contact
name & email
extra
TMs
FAPAS PROGRAMME & PROFICIENCY TEST ORDER FORM
APRIL 2012 – MARCH 2013
Veteriner İlaç Kalıntıları
dispatch
date
test details
place order
approx. 
quantity
dd/mm/yyyy
code
matrix
analyte
16/04/2012
02185
fish muscle
leucomalachite green & total malachite green
20 g
01/05/2012
#
honey
tetracyclines
20 g

15/05/2012
29/05/2012
25/06/2012
09/07/2012
30/07/2012
06/08/2012
20/08/2012
04/09/2012
02186
prawns
chloramphenicol
20 g
#
pig kidney
sulfonamides
20 g
#
fish muscle
quinolones & fluoroquinolones
20 g
#
corned beef
avermectins
20 g
#
pig liver
β-agonists
20 g

honey
chloramphenicol
20 g
#
bovine muscle
tetracyclines
20 g

fish muscle
(oily fish)
leucomalachite green & total malachite green
20 g
02187
02188
02189
02190
02191
02192
02193
02194
sample contact
name & email
extra
TMs
Dipnotlar
#
test Liste A'da belirtilen analitlerin belirlenmesi ve miktar tayinlerini içerir.

testin süresi kısadır.
Testlerde belirtilen genel kategorilerdeki muhtemel ilaç kalıntılarının listesi - Liste A.
tetracyclines chlortetracycline (total), doxycycline, oxytetracycline (total), tetracycline (total)
nitrofurans AHD (bound), AHD (total), AOZ (bound), AOZ (total), AMOZ (bound), AMOZ (total), SEM (bound), SEM (total)
sulfonamides sulfachloropyridazine, sulfadiazine, sulfadimethoxine, sulfadimidine (sulfamethazine), sulfadoxine, sulfaguanadine,
sulfamerazine, sulfamethizole, sulfamethoxazole, sulfamethoxypyridazine, sulfamonomethoxine, sulfamoxole,
sulphanilamide, sulfapyridine, sulfaquinoxaline, sulfathiazole, sulfisoxazole
quinolones & fluoroquinolones flumequine, nalidixic acid, oxolinic acid, ciprofloxacin, danofloxacin, difloxacin, enrofloxacin, marbofloxacin, norfloxacin,
sarafloxacin
avermectins abamectin, doramectin, emamectin, eprinomectin, ivermectin, moxidectin
β-agonists bromobuterol, cimaterol, cimbuterol, clenbuterol, clenpenterol , hydroxyclenbuterol, mabuterol, mapenterol,
ractopamine, salbutamol, salmeterol, terbutaline, tulobuterol, zilpaterol
synthetic hormones α-boldenone, methylboldenone, diethylstilbestrol (DES), dienestrol, hexoestrol, methyltestosterone, α-nortestosterone,
stanozolol, 16β-hydroxystanozolol, trenbolone, zeranol
nonsteroidal anti-inflammatory diclofenac, 5-hydroxyflunixin, ibuprofen, meloxicam, naproxen, phenylbutazone
drugs (NSAIDs)
coccidiostats decoquinate,diclazuril, halofuginone, lasalocid, maduramycin, monensin, narasin, DNC, robenidine, salinomycin,
semduramycin, toltrazuril sulfone
anthelmintics albendazole sulfone, albendazole-2-amino-sulfone, albendazole sulfoxide, total albendazole sulfone, closantel,
fenbantel, fenbendazole, oxfendazole, oxfendazole sulfone, total oxfendazole sulfone, flubendazole, levamisole,
mebendazole, hydroxymebendazole, mebendazole amine, total mebendazole, nitroxynil, thiabendazole, triclabendazole,
triclabendazole sulfone, triclalbendazole sulfoxide, ketotriclabendazole, total triclabendazole sulfone
thyrostats 6-methyl-2-thiouracil, dimethylthiouracil, ethylthiouracil, methimazole, mercaptobenzimidazole, tapazole, thiouracil,
methylthiouracil, phenylthiouracil, propylthiouracil
beta-lactams amoxicillin , ampicillin , benzylpenicillin (Penicillin G), Penicillin V, cloxacillin , dicloxacillin , nafpicillin , oxacillin,
cefalexin, cefalonium, cefapirin, desacetylcefapirin, cefazolin cefoperazone, cefquinome
®
FAPAS 2012-13 (Program) – Rev: 20111116
Sayfa 4 / 18
FAPAS PROGRAMME & PROFICIENCY TEST ORDER FORM
APRIL 2012 – MARCH 2013
Veteriner İlaç Kalıntıları (devam)
dispatch
date
test details
place order
approx. 
quantity
dd/mm/yyyy
code
matrix
analyte
25/09/2012
02195#
honey
sulfonamides
20 g
bovine milk
NSAIDs
(nonsteroidal anti-inflammatory drugs)
20 mL
chicken muscle
coccidiostats
20 g
#
08/10/2012
02196
30/10/2012
02197 #
06/11/2012
#
27/11/2012
08/01/2013
chicken eggs
nitrofuran metabolites
20 g
#
bovine urine
synthetic hormones & thyrostats
25 mL
#
chicken eggs
quinolones & fluoroquinolones
20 g
#
prawns
nitrofuran metabolites
20 g
02198
02199
02200
29/01/2013
02201
11/02/2013
02202
bovine milk
chloramphenicol & thiamphenicol
20 mL
05/03/2013
#
bovine milk
anthelmintics
20 mL
#
bovine milk
beta-lactams (penicillins & cephalosporins)
& dihydrostreptomycin
40 mL
26/03/2013
02204
02205
sample contact
name & email
extra
TMs
Dipnotlar
#
test Liste A'da belirtilen analitlerin belirlenmesi ve miktar tayinlerini içerir.

testin süresi kısadır.
Testlerde belirtilen genel kategorilerdeki muhtemel ilaç kalıntılarının listesi - Liste A.
tetracyclines chlortetracycline (total), doxycycline, oxytetracycline (total), tetracycline (total)
nitrofurans AHD (bound), AHD (total), AOZ (bound), AOZ (total), AMOZ (bound), AMOZ (total), SEM (bound), SEM (total)
sulfonamides sulfachloropyridazine, sulfadiazine, sulfadimethoxine, sulfadimidine (sulfamethazine), sulfadoxine, sulfaguanadine,
sulfamerazine, sulfamethizole, sulfamethoxazole, sulfamethoxypyridazine, sulfamonomethoxine, sulfamoxole,
sulphanilamide, sulfapyridine, sulfaquinoxaline, sulfathiazole, sulfisoxazole
quinolones & fluoroquinolones flumequine, nalidixic acid, oxolinic acid, ciprofloxacin, danofloxacin, difloxacin, enrofloxacin, marbofloxacin, norfloxacin,
sarafloxacin
avermectins abamectin, doramectin, emamectin, eprinomectin, ivermectin, moxidectin
β-agonists bromobuterol, cimaterol, cimbuterol, clenbuterol, clenpenterol , hydroxyclenbuterol, mabuterol, mapenterol,
ractopamine, salbutamol, salmeterol, terbutaline, tulobuterol, zilpaterol
synthetic hormones α-boldenone, methylboldenone, diethylstilbestrol (DES), dienestrol, hexoestrol, methyltestosterone, α-nortestosterone,
stanozolol, 16β-hydroxystanozolol, trenbolone, zeranol
nonsteroidal anti-inflammatory diclofenac, 5-hydroxyflunixin, ibuprofen, meloxicam, naproxen, phenylbutazone
drugs (NSAIDs)
coccidiostats decoquinate,diclazuril, halofuginone, lasalocid, maduramycin, monensin, narasin, DNC, robenidine, salinomycin,
semduramycin, toltrazuril sulfone
anthelmintics albendazole sulfone, albendazole-2-amino-sulfone, albendazole sulfoxide, total albendazole sulfone, closantel,
fenbantel, fenbendazole, oxfendazole, oxfendazole sulfone, total oxfendazole sulfone, flubendazole, levamisole,
mebendazole, hydroxymebendazole, mebendazole amine, total mebendazole, nitroxynil, thiabendazole, triclabendazole,
triclabendazole sulfone, triclalbendazole sulfoxide, ketotriclabendazole, total triclabendazole sulfone
thyrostats 6-methyl-2-thiouracil, dimethylthiouracil, ethylthiouracil, methimazole, mercaptobenzimidazole, tapazole, thiouracil,
methylthiouracil, phenylthiouracil, propylthiouracil
beta-lactams amoxicillin , ampicillin , benzylpenicillin (Penicillin G), Penicillin V, cloxacillin , dicloxacillin , nafpicillin , oxacillin,
cefalexin, cefalonium, cefapirin, desacetylcefapirin, cefazolin cefoperazone, cefquinome
®
FAPAS 2012-13 (Program) – Rev: 20111116
Sayfa 5 / 18
FAPAS PROGRAMME & PROFICIENCY TEST ORDER FORM
APRIL 2012 – MARCH 2013
Yem Maddeleri
Yem maddeleri ile ilgili 04197, 04204, 04207, 17120, 2288, 2289, 2291 ve 3036 testlerinin de bulunduğunu dikkate
alınız.
dispatch
date
test details
place order
approx. 
quantity
dd/mm/yyyy
code
matrix
analyte
17/05/2012
10101
dairy ration
moisture, ash, total oil, protein & crude fibre
150 g
17/05/2012
10102
dairy ration
iron, lead, magnesium, manganese & selenium
150 g
28/06/2012
10103
sheep feed
moisture, ash, total oil, protein & copper
150 g
06/09/2012
10104
pig ration
moisture, ash, total oil, protein, crude fibre, vitamin E
& zinc
150 g
09/11/2012
10105
poultry ration
moisture, ash, total oil, protein & crude fibre
150 g
09/11/2012
10106
poultry ration
starch, total sugars, calcium & phosphorus
150 g
14/02/2013
10107
premix
calcium, manganese, magnesium, phosphorus,
sodium & zinc
150 g
14/02/2013
10108
premix
vitamin A, D3, E
150 g
sample contact
name & email
extra
TMs
Allerjenler
Histamin ve sülfitler DIŞINDA (genellikle HPLC metotları kullanılır), sonuçlar ELISA kitlerinin markasına göre
gruplandırılarak değerlendirilir.
dispatch
date
test details
dd/mm/yyyy
code
13/04/2012
27103
03/05/2012
30/05/2012
place order
approx. 
quantity
matrix
analyte
infant soya
formula
milk
2 x 20 g
27104
cake mix
egg, egg white protein
2 x 20 g
27105
canned fish
histamine (high level)
145 g
infant soya
formula
gluten
2 x 20 g
§
§
§
27/06/2012
27106
27/07/2012
27107
02/08/2012
27108
24/08/2012
05/09/2012
§
chocolate
peanut, peanut protein
2 x 20 g
infant soya
formula
milk
2 x 20 g
27109
cake mix
gluten
2 x 20 g
27110
canned fish
histamine (low level)
145 g
§
§
sample contact
name & email
Dipnotlar
total sugars = titrasyon metodu sonucu (ör. Layne-Eynon, Luff-Schoorl, Munson Walker) veya HPLC ile yapıldıysa,
fruktoz, glikoz, sakkaroz, laktoz, galaktoz ve maltoz toplamı.
§
iki adet test materyali gönderilir. Kalitatif ve kantitatif sonuçlar bildirilebilir.
‡ Kalitatif ve kantitatif sonuçlar bildirilebilir.
/continued
®
FAPAS 2012-13 (Program) – Rev: 20111116
Sayfa 6 / 18
extra
TMs
FAPAS PROGRAMME & PROFICIENCY TEST ORDER FORM
APRIL 2012 – MARCH 2013
Allerjenler (devam)
Histamin ve sülfitler DIŞINDA (genellikle HPLC metotları kullanılır), sonuçlar ELISA kitlerinin markasına göre
gruplandırılarak değerlendirilir.
dispatch
date
test details
dd/mm/yyyy
code
21/09/2012
23/10/2012
31/10/2012
21/11/2012
place order
approx. 
quantity
matrix
analyte
27111
chocolate
hazelnut, hazelnut protein
2 x 20 g
27112
jam
sulphites
20 g
cake mix
gluten, milk and egg
30 g
wheat flour
soya, soya protein
2 x 20 g
§
‡
27113
§
27114
♦
02/01/2013
27115
chocolate
contamination (presence/absence) of matrix with one
or more from the following list:
Almond, (Amygdalus communis L.)
Hazelnut, (Corylus avellana)
Walnut, (Juglans regia)
Cashew, (Anacardium occidentale)
Pecan nut, (Carya illinoiesis (Wangenh.) K. Koch))
Brazil nut, (Bertholletia excels)
Pistachio nut, (Pistacia vera)
Macadamia / Queensland nut (Macadamia ternifolia)
50 g
07/02/2013
27116
canned fish
histamine (high level)
145 g
chocolate
almond, almond protein
2 x 20 g
07/03/2013
§
27117
sample contact
name & email
extra
TMs
Çevresel Bulaşanlar
dispatch
date
test details
place order
approx. 
quantity
dd/mm/yyyy
code
matrix
analyte
20/04/2012
0651
palm oil
PAHs
30 mL
02/10/2012
0652
smoked meat
product
PAHs
50 g
07/02/2013
0653
olive oil
all 16 EU priority PAHs
30 mL
Dipnotlar
§
iki adet test materyali gönderilir. Kalitatif ve kantitatif sonuçlar bildirilebilir.
‡ Kalitatif ve kantitatif sonuçlar bildirilebilir.
♦ sadece kalitatif sonuçlar
®
FAPAS 2012-13 (Program) – Rev: 20111116
Sayfa 7 / 18
sample contact
name & email
extra
TMs
FAPAS PROGRAMME & PROFICIENCY TEST ORDER FORM
APRIL 2012 – MARCH 2013
Migrasyon – Overall & Specific
dispatch
date
test details
place order
approx. 
quantity
dd/mm/yyyy
code
matrix
analyte
26/04/2012
1144
nylon film
overall migration into ethanol by total immersion
40 cm x
22 cm
08/11/2012
1145
plastic film
overall migration into olive oil by total immersion
40 cm x
22 cm
21/06/2012
1250
food stimulant
phthalates
2 x 50 mL
melamine
50 mL
bisphenol A
50 mL
formaldehyde
50 mL
total primary aromatic amines
>300 mL
photo initiators
2 x 50 mL
B
sample contact
name & email
extra
TMs
(oil)
19/07/2012
1251
food simulant
(3% w/v acetic acid
in water)
15/08/2012
1252
food simulant
(50% w/v ethanol)
06/09/2012
1253
food stimulant
(3% w/v acetic acid
in water)
23/11/2012
1254
food simulant
(3% w/v acetic acid
in water)
28/02/2013
1255
B
food stimulant
(oil)
Besin Elementleri
dispatch
date
test details
place order
approx. 
quantity
dd/mm/yyyy
code
matrix
analyte
04/04/2012
1867
canned meat
calcium, phosphorus & zinc (all natural levels)
150 g
05/07/2012
1868
breakfast cereal
calcium, iron & zinc (fortified)
50 g
14/11/2012
1869
milk powder
calcium, iodine & selenium (all natural levels)
50 g
22/02/2013
1870
energy drink
iron, magnesium, manganese, potassium, selenium
(all natural levels)
50 g
Dipnotlar
B
Blank matriks dahildir.
®
FAPAS 2012-13 (Program) – Rev: 20111116
Sayfa 8 / 18
sample contact
name & email
extra
TMs
FAPAS PROGRAMME & PROFICIENCY TEST ORDER FORM
APRIL 2012 – MARCH 2013
Mikotoksinler – Aflatoksin
04192, 04201, 04204 ve 04209 ELISA taramaları yapan laboratuvarlara yöneliktir.
dispatch
date
test details
place order
approx. 
quantity
dd/mm/yyyy
code
matrix
analyte
11/04/2012
04192
maize
aflatoxin B1, DON, ZON & OTA
150 g
24/04/2012
04193
pistachio
aflatoxins B & G &/or total
100 g
(water/nut slurry)
10/05/2012
04194
maize
aflatoxins B & G &/or total
55 g
18/05/2012
04195
milk powder
aflatoxin M1
55 g
20/06/2012
04196
chilli powder
aflatoxins B & G &/or total
55 g
04/07/2012
04197
animal feed
aflatoxins B & G &/or total
55 g
(cereal based)
25/07/2012
04198
peanut
aflatoxins B & G &/or total
55 g
07/08/2012
04199
infant food
contamination of matrix with one or more from the
following list: aflatoxins B & G &/or total, OTA, ZON,
DON, FB1 & FB2 & total fumonisins (as a sum of FB1 &
FB2)
150 g
21/08/2012
04200
almond
aflatoxins B & G &/or total
100 g
aflatoxin B1, DON, ZON & OTA
150 g
(water/nut slurry)
07/09/2012
04201
maize
26/09/2012
04202
milk powder
aflatoxin M1
55 g
16/10/2012
04203
hazelnut
aflatoxins B & G &/or total
100 g
24/10/2012
04204
contamination of matrix with one or more from the
following list: aflatoxin B1, OTA, ZON & DON
150 g
(cereal based)
(water/nut slurry)
animal feed
07/11/2012
04205
maize
aflatoxins B & G &/or total
55 g
28/11/2012
04206
mixed spice
aflatoxins B & G &/or total
55 g
07/12/2012
04207
animal feed
aflatoxins B & G &/or total
55 g
aflatoxins B & G &/or total
100 g
(cereal based)
08/01/2013
04208
pistachio
(water/nut slurry)
23/01/2013
04209
maize
aflatoxin B1, DON, ZON & OTA
150 g
31/01/2013
04210
rice
aflatoxins B & G &/or total
55 g
08/02/2013
04211
peanut
aflatoxins B & G &/or total
55 g
25/02/2013
04212
dried figs
aflatoxins B & G &/or total
100 g
aflatoxin M1
55 g
(water/fruit slurry)
23/03/2013
04213
milk powder
®
FAPAS 2012-13 (Program) – Rev: 20111116
Sayfa 9 / 18
sample contact
name & email
extra
TMs
FAPAS PROGRAMME & PROFICIENCY TEST ORDER FORM
APRIL 2012 – MARCH 2013
Mikotoksinler – Patulin
dispatch
date
test details
place order
approx. 
quantity
dd/mm/yyyy
code
matrix
analyte
19/06/2012
1647
apple juice
patulin
50 mL
sample contact
name & email
extra
TMs
(clear)
18/09/2012
1648
apple purée
patulin
60 g
19/02/2013
1649
apple juice
patulin
50 mL
(cloudy)
Mikotoksinler – Okratoksin A
OTA ile ilgili 04199, 04201, 04204 ve 04209 roundlarının da bulunduğunu dikkate alınız.
dispatch
date
test details
place order
approx. 
quantity
dd/mm/yyyy
code
matrix
analyte
04/05/2012
17111
wheat flour
ochratoxin A
55 g
29/05/2012
17112
dried vine fruit
ochratoxin A
100 g
sample contact
name & email
extra
TMs
(water/fruit slurry)
06/07/2012
17113
barley flour
ochratoxin A
55 g
09/08/2012
17114
green coffee
ochratoxin A
55 g
13/09/2012
17115
paprika
ochratoxin A
55 g
26/10/2012
17116
instant coffee
ochratoxin A
55 g
04/12/2012
17117
wine
ochratoxin A
55 mL
10/01/2013
17118
maize flour
ochratoxin A
55 g
08/02/2013
17119
roasted coffee
ochratoxin A
55 g
28/02/2013
17120
animal feed
ochratoxin A
55 g
21/03/2013
17121
cocoa
ochratoxin A
55 g
Mikotoksinler – Fusarium toksinleri
Fusarium toksinleri içerebilecek 4199, 04201, 04204 ve 04209 roundlarının olduğunu da dikkate alınız.
dispatch
date
test details
place order
approx. 
quantity
dd/mm/yyyy
code
matrix
analyte
18/04/2012
2283
maize flour
deoxynivalenol (DON)
55 g
06/06/2012
2284
breakfast cereal
zearalenone (ZON)
55 g
06/06/2012
2285
breakfast cereal
deoxynivalenol (DON)
55 g
28/06/2012
2286
oat flour
T-2 & HT-2 toxins
55 g
18/07/2012
2287
maize flour
FB1 & FB2 and total fumonisins
(as a sum of FB1 & FB2)
55 g
01/11/2012
2288
animal feed
zearalenone (ZON)
55 g
01/11/2012
2289
animal feed
deoxynivalenol (DON)
55 g
30/01/2013
2290
wheat flour
deoxynivalenol (DON)
55 g
08/03/2013
2291
animal feed
T-2 & HT-2 toxins
55 g
®
FAPAS 2012-13 (Program) – Rev: 20111116
Sayfa 10 / 18
sample contact
name & email
extra
TMs
FAPAS PROGRAMME & PROFICIENCY TEST ORDER FORM
APRIL 2012 – MARCH 2013
Vitaminler
dispatch
date
test details
place order
approx. 
quantity
dd/mm/yyyy
code
matrix
analyte
24/05/2012
2176
breakfast cereal
vitamins B1, B2 (total) & B6, total niacin &
total folate
50 g
13/07/2012
2177
fruit purée
vitamin C
100 mL
20/11/2012
2178
liquid vitamin
supplement
vitamins B1, B2 (total) & B6
40 mL
17/01/2013
2179
milk powder
vitamins A & D3
50 g
13/03/2013
2180
powdered baby
food
vitamins A, B12, C & E
50 g
sample contact
name & email
extra
TMs
Bileşen / Katkı maddeleri
dispatch
date
test details
place order
approx. 
quantity
dd/mm/yyyy
code
matrix
analyte
04/04/2012
2091
tomato sauce
brix, pH, total acidity, sodium & chloride
150 g
08/05/2012
2092
meat
sulphur dioxide
100 g
01/06/2012
2093
jam
brix, pH, benzoic acid, citric acid & sorbic acid
50 g
08/08/2012
2094
chocolate cake
mix
caffeine, sorbic acid, theobromine &
total sugars (expressed as sucrose)
50 g
11/09/2012
2095
dried apricot
sulphur dioxide
100 g
permitted colours
50 g
sample contact
name & email
(water/fruit slurry)
17/10/2012
2096
§
sugar
confectionary
(boiled sweets)
05/12/2012
2097
20/02/2013
2098
§
up to 4 selected from the following list:
Allura Red, Brilliant Blue FCF, Carmoisine, Erythrosine,
Green S, Indigo Carmine,
Patent Blue V, Ponceau 4R, Quinoline Yellow, Sunset
Yellow FCF, Tartrazine
oil
antioxidants: total BHA (E320), BHT (E321) & propyl
gallate (E310)
50 mL
hot pepper sauce
non-permitted colours (illegal dyes)
50 mL
(or similar)
up to 4 selected from the following list:
Butter Yellow (Dimethyl Yellow), Orange II,
Para Red, Rhodamine B, Sudan I, Sudan II,
Sudan III, Sudan IV, Sudan Black B,
Sudan Orange G, Sudan Red B, Sudan Red 7B,
Sudan Red G, Toluidine Red
Dipnotlar
total sugars = titrasyon metodu sonucu (ör. Layne-Eynon, Luff-Schoorl, Munson Walker) veya HPLC ile yapıldıysa,
fruktoz, glikoz, sakkaroz, laktoz, galaktoz ve maltoz toplamı.

§
testin süresi kısadır.
Kalitatif ve kantitatif sonuçlar bildirilebilir
®
FAPAS 2012-13 (Program) – Rev: 20111116
Sayfa 11 / 18
extra
TMs
FAPAS PROGRAMME & PROFICIENCY TEST ORDER FORM
APRIL 2012 – MARCH 2013
Metalik Bulaşanlar
dispatch
date
test details
place order
dd/mm/yyyy
code
matrix
analyte
19/04/2012
07172
milk powder
arsenic, cadmium, mercury & lead
approx. 
quantity
50 g
(all natural / low levels)
16/05/2012
07173
soft drink
antimony, arsenic (total) cadmium, chromium copper
& zinc (all high levels)
50 mL
14/06/2012
07174
canned fish
arsenic (total), cadmium & mercury (total)
150 g
(all natural levels)
26/06/2012
07175
tomato paste
cadmium, lead, iron & tin
50 g
(all high levels)
18/07/2012
07176
chilli powder
arsenic (total), cadmium & lead
50 g
(all high levels)
03/08/2012
07177
infant formula
aluminium, chromium, molybdenum, selenium
50 g
(all natural / low levels)
29/08/2012
07178
canned crab
meat
arsenic (total), arsenic (inorganic), cadmium, lead &
mercury (total)
150 g
(all natural levels)
19/09/2012
07179
chilli sugar paste
lead
25 g
28/09/2012
07180
edible oil
arsenic (total), copper, iron & lead
50 mL
(all high levels)
04/10/2012
07181
wine
pH, cadmium & lead
50 mL
25/10/2012
07182
canned fish
arsenic (total), cadmium, mercury (total)
150 g
(all natural levels)
21/11/2012
07183
infant cereal
cadmium, chromium, lead, mercury (total) & selenium
50 g
(all natural / low levels)
11/12/2012
07184
soya flour
16/01/2013
07185
cocoa powder
aluminium, arsenic (total), cadmium, lead & mercury
(total) (all high levels)
50 g
cadmium & lead
50 g
(both natural levels)
05/02/2013
07186
fruit juice
cadmium, iron, lead, & tin (all high levels)
50 mL
20/02/2013
07187
powdered rice
arsenic (inorganic), arsenic (total) & cadmium
50 g
(all high levels)
19/03/2013
07188
vegetable purée
cadmium, lead & tin (all high levels)
50 g
27/03/2013
07189
canned fish
arsenic (total), methyl mercury &
mercury (total)
150 g
(all natural levels)
®
FAPAS 2012-13 (Program) – Rev: 20111116
Sayfa 12 / 18
sample contact
name & email
extra
TMs
FAPAS PROGRAMME & PROFICIENCY TEST ORDER FORM
APRIL 2012 – MARCH 2013
Meyve Suyu, Alkollü ve Alkolsüz İçecekler
dispatch
date
test details
place order
approx. 
quantity
dd/mm/yyyy
code
matrix
analyte
31/05/2012
0844
apple juice
brix, pH, total acidity, total sugars,
magnesium, potassium & sodium
250 mL
11/10/2012
0845
orange juice
brix, pH, citric acid,
sucrose, glucose, fructose & total sugars
250 mL
03/01/2013
0846
grapefruit juice
brix, pH, total acidity, total sugars,
calcium, magnesium & potassium
250 mL
14/03/2013
0847
cranberry juice
brix, pH, total acidity, total sugars,
phosphorus & potassium
250 mL
04/05/2012
03103
cola drink
benzoic acid, caffeine,
acesulfame-K & saccharin
150 mL
12/07/2012
03104
ground coffee
caffeine
2 x 30 g
sample contact
name & email
(2 test materials supplied,
one regular, one decaffeinated)
22/08/2012
03105
10/10/2012
03106
§
soft drink
soft drink
brix, pH, citric acid, sorbic acid,
cyclamate & saccharin
150 mL
up to 4 colours from the following list:
150 mL
Allura Red, Brilliant Blue FCF, Carmoisine, Erythrosine,
Green S, Indigo Carmine,
Patent Blue V, Ponceau 4R, Quinoline Yellow,
Sunset Yellow FCF, Tartrazine
29/11/2012
03107
cola drink
caffeine, benzoic acid, total sugars &
phosphoric acid (as P2O5)
150 mL
13/02/2013
03108
tonic water
benzoic acid, quinine,
acesulfame-K & aspartame
150 mL
10/05/2012
1365
whisky
alcoholic strength, ethanol (acetaldehyde), ethyl
acetate, methanol, propan-1-ol, 2-methylpropanol &
2-methylbutanol + 3-methylbutanol (sum)
200 mL
12/09/2012
1366
brandy
alcoholic strength, ethanol (acetaldehyde), ethyl
acetate, methanol, propan-1-ol, 2-methylpropanol &
2-methylbutanol + 3-methylbutanol (sum) & ethyl
carbamate
200 mL
06/02/2013
1367
wine
alcoholic strength, total SO2, total acidity & volatile
acidity
220 mL
Footnotes
Dipnotlar
total sugars = titrasyon metodu sonucu (ör. Layne-Eynon, Luff-Schoorl, Munson Walker) veya HPLC ile yapıldıysa,
fruktoz, glikoz, sakkaroz, laktoz, galaktoz ve maltoz toplamı.
§
Kalitatif ve kantitatif sonuçlar bildirilebilir.
®
FAPAS 2012-13 (Program) – Rev: 20111116
Sayfa 13 / 18
extra
TMs
FAPAS PROGRAMME & PROFICIENCY TEST ORDER FORM
APRIL 2012 – MARCH 2013
Sıvı ve Katı Yağlar
dispatch
date
test details
place order
approx. 
quantity
dd/mm/yyyy
code
matrix
analyte
17/04/2012
14111
nutritionally
fortified oil
saturates, mono-unsaturates,
poly-unsaturates, total trans fatty acids & individual
fatty acids
30 mL
total fat, saturates, mono-unsaturates,
poly-unsaturates, total trans fatty acids &
individual fatty acids
50 g
(may contain
LC-PUFAs)
09/05/2012
14112
infant formula
(may contain
encapsulated
LC-PUFAs)
22/05/2012
14113
olive oil
peroxide value, acidity, anisidine value & iodine value
100 mL
11/07/2012
14114
cereal product
total fat, saturates, mono-unsaturates,
poly-unsaturates, total trans fatty acids &
individual fatty acids
50 g
(may contain
encapsulated
LC-PUFAs)
27/07/2012
14115
vegetable oil
saturates, mono-unsaturates,
poly-unsaturates & total trans fatty acids (& possibly
individually specified fatty acids)
30 mL
14/08/2012
14116
mixed fat spread
total fat, saturates, mono-unsaturates,
poly-unsaturates, & trans fatty acids
50 g
09/10/2012
14117
olive oil
peroxide value, acidity, anisidine value &
iodine value
100 mL
18/10/2012
14118
fish oil
omega-3 & omega-6 series fatty acids
30 mL
27/11/2012
14119
mixed fat spread
total fat, butyric acid & cholesterol
50 g
06/02/2013
14120
vegetable oil
saturates, mono-unsaturates,
poly-unsaturates
30 mL
11/03/2013
14121
olive oil
peroxide value, acidity, K232 & K270
100 mL
Dipnotlar

testin süresi kısadır.
®
FAPAS 2012-13 (Program) – Rev: 20111116
Sayfa 14 / 18
sample contact
name & email
extra
TMs
FAPAS PROGRAMME & PROFICIENCY TEST ORDER FORM
APRIL 2012 – MARCH 2013
Pestisit Kalıntıkları – Hayvansal Ürünler / Katı ve Sıvı Yağlar
Her test materyali (0588 hariç) Liste 1’de belirtilen pestisitlerden birkaç tanesini içerir.
dispatch
date
test details
place order
approx. 
quantity
dd/mm/yyyy
code
matrix
analyte
25/04/2012
0582
hydrogenated
vegetable oil
selection from List 1
25 g
0582b
blank hydrogenated
vegetable oil
BLANK
(only available if ordered with test 0582)
25 g
23/05/2012
0583
milk powder
selection from List 1
50 g
20/07/2012
0584
olive oil
selection from List 1
50 g
20/09/2012
0585
hydrogenated
vegetable oil
selection from List 1
25 g
0585b
blank hydrogenated
vegetable oil
BLANK
(only available if ordered with test 0585)
25 g
13/11/2012
0586
oily fish
selection from List 1
50 g
22/01/2013
0587
animal (pork) fat
selection from List 1
50 g
12/03/2013
0588
fish muscle
trifluralin (single herbicide)
20 g
sample contact
name & email
Potansiyel pestisit kalıntıları (belirtilmediği sürece sadece ana madde) – Liste 1
aldrin
cypermethrin
fenpropimorph
haloxyfop
quintozene
azinphos-ethyl
pp-DDE
fenthion
cis-heptachlor epoxide
prochloraz
bifenthrin
pp-DDD (TDE)
fenthion sulfone
trans-heptachlor epoxide
tebuconazole
boscalid
op-DDT
fenthion sulfoxide
methacrifos
tecnazene
cis-chlordane
pp’-DDT
fenvalerate
methidathion
triazophos
trans-chlordane
deltamethrin
fluazifop
4,4’-methoxychlor
vinclozolin
oxychlordane
diazinon
fluquinconazole
nitrofen
PCB 28
chlorfenvinphos
dieldrin
flusilazole
parathion-ethyl
PCB 52
chlorobenzilate
alpha-endosulfan (endosulfan I)
formothion
parathion-methyl
PCB 101
chlorpropham
beta-endosulfan (endosulfan II)
hexachlorobenzene (HCB)
pendimethalin
PCB 118
chlorpyrifos (-ethyl)
endosulfan sulfate
alpha-hexachlorocyclohexane (-HCH)
permethrin (sum isomers)
PCB 138
chlorpyrifos-methyl
endrin
beta-hexachlorocyclohexane (-HCH)
pirimiphos-methyl
PCB 153
cyfluthrin (sum isomers)
epoxiconazole
gamma- hexachlorocyclohexane (lindane)
profenofos
PCB 180
lambda-cyhalothrin
famoxadone
heptachlor
pyrazophos
®
FAPAS 2012-13 (Program) – Rev: 20111116
Sayfa 15 / 18
extra
TMs
FAPAS PROGRAMME & PROFICIENCY TEST ORDER FORM
APRIL 2012 – MARCH 2013
Pestisit Kalıntıları – Tahıl Ürünleri
Her test materyali (0978 hariç) Liste 2'de belirtilen pestisitlerden birkaç tanesini içerir.
dispatch
date
test details
place order
approx. 
quantity
dd/mm/yyyy
code
matrix
analyte
11/05/2012
0976
maize flour
selection from list 2
50 g
24/07/2012
0977
wheat flour
selection from list 2
50 g
0977b
blank wheat flour
BLANK
(only available if ordered with test 0977)
50 g
05/09/2012
0978
cereal
chlormequat (single pesticide)
50 g
03/10/2012
0979
brown rice
selection from List 2
50 g
22/11/2012
0980
baby food
selection from List 2
50 g
06/03/2013
0981
wheat flour
selection from list 2
50 g
0981b
blank wheat flour
BLANK
(only available if ordered with test 0981)
50 g
sample contact
name & email
extra
TMs
Potansiyel pestisit kalıntıları (belirtilmediği sürece sadece ana madde) – Liste 2
acephate
deltamethrin
fenthion sulfone
malathion
pyrimethanil
azinphos-methyl
demeton-S-methyl sulfone
fenpropimorph
methacrifos
quintozene
azoxystrobin
diazinon
fenvalerate(sum of isomers)
methomyl
spiroxamine
bifenthrin
dichlorvos
fipronil
omethoate
tebuconazole
bromophos-ethyl
difenoconazole
fludioxonil
oxydemeton-methyl
(demeton-S-methyl sulfoxide)
tebufenozide
captan
diflubenzuron
fluquinconazole
paclobutrazole
terbufos
carbaryl
dimethoate
flusilazole
parathion-ethyl
terbufos sulfoxide
carbendazim
dimoxystrobin
flutriafol
penconazole
terbufos sulfone
carbofuran
disulfoton
formothion
pendimethalin
tetrachlorvinphos
3-hydroxycarbofuran
alpha-endosulfan (endosulfan I)
alpha-hexachlorocyclohexane
(-HCH)
permethrin (sum)
thiabendazole
carboxin
beta-endosulfan (endosulfan II)
beta-hexachlorocyclohexane
(-HCH)
phorate
thiacloprid
chlorfenvinphos
endosulfan sulfate
gamma-HCH (lindane)
phorate sulfoxide
thiamethoxam
chlorothalonil
epoxiconazole
hexaconazole
phorate sulfone
thiodicarb
chlorpropham
ethion
imazalil
phosalone
triadimefon
chlorpyrifos
ethoprophos
imidacloprid
phosmet
triadimenol
chlorpyrifos-methyl
etrimphos
iprodione
phosphamidon
(sum of isomers)
triazophos
clothianidin
fenamiphos
isofenphos-methyl
pirimicarb
tricyclazole
cyfluthrin (sum of isomers)
fenamiphos sulfoxide
isoprothiolane
desmethyl-pirimicarb
trifloxystrobin
lambda-cyhalothrin
fenamiphos sulfone
isoproturon
pirimiphos-methyl
trifluralin
cypermethrin
fenbuconazole
kresoxim-methyl
prochloraz
triticonazole
cyproconazole
fenhexamid
linuron
pyraclostrobin
vinclozolin
cyprodinil
fenitrothion
malaoxon
pyridaphenthion
disulfoton sulfoxide
fenthion
metconazole
procymidone
disulfoton sulfone
fenthion sulfoxide
metribuzin
propiconazole
®
FAPAS 2012-13 (Program) – Rev: 20111116
Sayfa 16 / 18
FAPAS PROGRAMME & PROFICIENCY TEST ORDER FORM
APRIL 2012 – MARCH 2013
Pestisit Kalıntıları – Taze ve kuru meyveler, Taze sebzeler, Çay ve aromatik otlar
Meyve, sebze ve aromatic ot matriksleri taze meyve, sebze veya otların püre haline getirilmesiyle hazırlanacaktır.
Herbir test materyali (19145 hariç) Liste 3'te belirtilen pestisitlerden birkaçını içerir. 19145 Liste 4'te belirtilen
pestisitlerden birkaçını içerir.
dispatch
date
test details
dd/mm/yyyy
code
30/04/2012
19133P
P
19133b
30/04/2012
19134
P
P
19134b
28/05/2012
19135
P
pesticide residues from List 3
90 g
blank lemon
BLANK
90 g
tomato
pesticide residues from List 3
90 g
blank dried vine fruit
(raisin)
BLANK
90 g
90 g
19137
P
19138
P
19139
P
19140
P
19141
P
19142
P
P
19142b
19143
P
19143bP
14/01/2013
90 g
lemon
90 g
19141b P
14/01/2013
90 g
90 g
19140bP
26/11/2012
BLANK
BLANK
19139bP
26/11/2012
pesticide residues from List 3
pesticide residues from List 3
19138bP
22/10/2012
apple
blank apple
blank tomato
19137b
22/10/2012
approx. 
quantity
dried vine fruit
(raisin)
P
17/09/2012
analyte
P
19136
19136bP
17/09/2012
matrix
P
19135b
28/05/2012
place order
19144
P
strawberry
pesticide residues from List 3
blank strawberry
BLANK
90 g
sweet (bell)
pepper
pesticide residues from List 3
90 g
blank sweet (bell)
pepper
BLANK
90 g
apricot
pesticide residues from List 3
90 g
blank apricot
BLANK
90 g
lettuce
pesticide residues from List 3
90 g
blank lettuce
BLANK
90 g
green beans
(inc. pods)
pesticide residues from List 3
90 g
blank green beans
(inc. pods)
BLANK
90 g
90 g
melon
pesticide residues from List 3
blank melon
BLANK
90 g
basil (herb)
pesticide residues from List 3
90 g
blank basil (herb)
BLANK
90 g
cabbage
pesticide residues from List 3
90 g
19144bP
blank cabbage
BLANK
90 g
18/01/2013
19145
tea
pesticide residues from List 4
50 g
19145b
blank tea
BLANK
50 g
18/02/2013
19146
grape
pesticide residues from List 3
90 g
P
19146bP
18/02/2013
19147
P
P
19147b
18/03/2013
19148
P
19148bP
18/03/2013
19149
P
19149bP
blank grape
BLANK
90 g
pear
pesticide residues from List 3
90 g
blank pear
BLANK
90 g
potato
pesticide residues from List 3
90 g
blank potato
BLANK
90 g
orange
pesticide residues from List 3
90 g
blank orange
BLANK
90 g
Footnotes
BLANK nuumuneler sadece ilgili yeterlik testi ile birlikte sipariş edilebilir
P
matriks püredir
®
FAPAS 2012-13 (Program) – Rev: 20111116
Sayfa 17 / 18
sample contact
name & email
extra
TMs
FAPAS PROGRAMME & PROFICIENCY TEST ORDER FORM
APRIL 2012 – MARCH 2013
Potansiyel pestisit kalıntıları (belirtilmediği sürece sadece ana madde) – Liste
2-phenylphenol
acephate
acetamiprid
acrinathrin
aldicarb
aldicarb sulfone
(aldoxycarb)
aldicarb sulfoxide
amitraz
atrazine
azinphos-methyl
cypermethrin
(sum of isomers)
cyproconazole
cyprodinil
pp’-DDD (TDE)
pp’-DDE
op’-DDT
pp’-DDT
deltamethrin
demeton-S-methyl sulfone
desmethyl-pirimicarb
diazinon
dichlofluanid
azoxystrobin
dichlorvos
bifenthrin
biphenyl
2,4-D
fenarimol
fenazaquin
fenbuconazole
fenhexamid
fenitrothion
fenoxycarb
fenpropathrin
fenpropimorph
fenpyroximate
fenthion
fenthion sulfoxide
fenthion sulfone
metaflumizone
(sum of isomers)
metalaxyl
metconazole
methamidophos
methidathion
methiocarb
methiocarb sulfone
methiocarb sulfoxide
methomyl
4,4’-methoxychlor
methoxyfenozide
monocrotophos
prothiofos
pymetrozine
pyraclostrobin
pyrazophos
pyrethrins (sum)
pyridaben
pyrimethanil
pyriproxyfen
quinalphos
quinoxyfen
quintozene
myclobutanil
dicloran
dicofol
(sum of isomers)
dicrotophos
diethofencarb
fenvalerate
(sum of isomers)
fipronil
fipronil sulfone
spinosad
(spinosyn A + spinosyn D)
spiroxamine
omethoate
oxadixyl
tebuconazole
tebufenozide
fluazifop-P-butyl (sum)
fludioxonil
tebufenpyrad
tecnazene
diethofencarb sulfoxide
diethofencarb sulfone
flufenoxuron
fluquinconazole
oxamyl
oxydemeton-methyl
(demeton-S-methyl sulfoxide)
oxyfluorfen
paclobutrazol
teflubenzuron
tefluthrin
difenoconazole
diflubenzuron
dimethoate
dimethomorph
(sum of isomers)
diniconazole
diphenylamine
DMST
flusilazole
flutriafol
folpet
formetanate HCl
paraoxon-methyl
parathion (-ethyl)
parathion-methyl
penconazole
terbufos
terbufos sulfoxide
terbufos sulfone
terbuthylazine
fosthiazate
haloxyfop (free acid)
HCB (hexachlorobenzene)
tetraconazole
tetradifon
thiabendazole
carbofuran
3-hydroxy carbofuran
chlorfenapyr
chlorfenvinphos
(sum of isomers)
chlorobenzilate
dodine
alpha-endosulfan
(endosulfan I)
beta-endosulfan
hexaconazole
hexythiazox
imazalil
imidacloprid
pencycuron
pendimethalin
permethrin
(sum of isomers)
phenthoate
phosalone
phosmet
phoxim
thiacloprid
thiamethoxam
thiodicarb
tolclofos-methyl
(endosulfan II)
pirimicarb
tolylfluanid
chlorothalonil
chlorpropham
chlorpyrifos (-ethyl)
chlorpyrifos-methyl
chlorthal-dimethyl
chlozolinate
clofentezine
clothianidin
cyfluthrin
(sum of isomers)
lambda-cyhalothrin
endosulfan sulfate
EPN
epoxiconazole
ethion
ethoprophos
etofenprox
famoxadone
fenamiphos
fenamiphos sulfone
indoxacarb
(sum isomers)
iprodione
iprovalicarb
isofenphos-methyl
isoprocarb
isoproturon
kresoxim-methyl
lenacil
linuron
lufenuron
pirimiphos-methyl
prochloraz (sum)
procymidone
profenofos
propamocarb
propaquizafop
propargite
propiconazole
propoxur
triadimefon
triadimenol
triazophos
trifloxystrobin
trifluralin
triticonazole
vinclozolin
zoxamide
fenamiphos sulfoxide
mepanipyrim
propyzamide
bitertanol
boscalid
bromopropylate
bromuconazole
(sum of isomers)
bupirimate
buprofezin
butocarboxim
butocarboxim sulfoxide
cadusafos
carbaryl
carbendazim
Potansiyel pestisit kalıntıları (belirtilmediği sürece sadece ana madde) – Liste 4
bifenthrin
chlorothalonil
chlorpyrifos (-ethyl)
lambda-cyhalothrin
cypermethrin (sum isomers)
deltamethrin
dicofol
dimethoate
pp’-DDD (TDE)
pp’-DDE
op’-DDT
pp’-DDT
alpha-endosulfan (endosulfan I)
beta-endosulfan (endosulfan II)
endosulfan sulfate
ethion
fenazaquin
fenitrothion
®
fenpropathrin
fenvalerate (sum isomers)
HCB (hexachlorobenzene)
phosalone
procymidone
propargite
FAPAS 2012-13 (Program) – Rev: 20111116
Sayfa 18 / 18
quinalphos
trifloxystrobin